NACE TM0498-2023 PDF

This AMPP standard establishes a standard test procedure for pack bed carburization of alloys used for ethylene manufacture. The pack bed carburization procedure is specified in this standard because it is simple to perform. The test specimen geometry chosen reflects the intent of the procedure to be used for evaluation of carburization of furnace tube alloys intended for ethylene manufacture.
This standard also establishes two recommended methods—combustion analysis and chemical etching—for measuring the relative carburization of alloys for tubes intended for service in ethylene manufacture, or for assessing the performance of these tubes after service. Application procedures for the two methods are defined in detail. The combustion analysis method is preferred because it is quantitative. The chemical etching method is simpler and less expensive, but is only semiquantitative. Other methods considered and the reasons they are not recommended are discussed in Appendix A (nonmandatory).
The carburization measurement methods in this standard may be used independently from the pack bed carburization procedure when assessing the condition of tubes after service or when other carburization procedures have been performed.
This standard is intended to assist designers, operators, producers, fabricators, users, and testing laboratories in the selection of furnace tube alloys used for ethylene manufacture.