Name:
ASTM D7598-16(2017) PDF
Published Date:
06/15/2017
Status:
Active
Publisher:
ASTM International
1.1 This procedure covers the determination of thiodiglycol (TDG) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). TDG is qualitatively and quantitatively determined by this test method. This test method adheres to single reaction monitoring (SRM) mass spectrometry.
1.2 This test method has been developed by U.S. EPA Region 5 Chicago Regional Laboratory (CRL).
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 The detection verification level (DVL) and reporting range for TDG are listed in Table 1.
| Analyte | DVL (μg/L) | Reporting Range (μg/L) |
| Thiodiglycol | 20 | 100-10 000 |
1.4.1 The DVL is required to be at a concentration at least 3 times below the reporting limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratio at the DVL.
FIG. 1 Example SRM Chromatograms Signal/Noise at Detection Verification Level
1.4.2 The RL is the concentration of the Level 1 calibration standard as shown in Table 2. The reporting limit for this test method is 100 μg/L.
| Analyte/Surrogate | LV 1 | LV 2 | LV 3 | LV 4 | LV 5 | LV 6 | LV 7 |
| Thiodiglycol | 100 | 250 | 500 | 1 000 | 2 500 | 5 000 | 10 000 |
| 3,3'-Thiodipropanol | 100 | 250 | 500 | 1 000 | 2 500 | 5 000 | 10 000 |
| File Size : | 1 file , 180 KB |
| Note : | This product is unavailable in Russia, Ukraine, Belarus |
| Number of Pages : | 9 |
| Published : | 06/15/2017 |
