In this research, gas chromatography/chemical ionization/tandem mass
spectrometry, coupled with direct aqueous derivatization, liquid-liquid extraction, and solid-phase
extraction techniques, has been optimized for the analysis of selected hydrazines. A
procedural calibration technique using an isotopically labeled internal standard was optimized
for the analysis of hydrazine. Direct aqueous derivatization with 3,5-
dinitrobenzoyl chloride was studied for the analysis of other selected hydrazines. The method
accuracy, precision, sensitivity, and matrix effects were studied. Includes abstract only.
| Edition : | Vol. - No. |
| File Size : | 1
file
, 71 KB |
| Note : | This product is unavailable in Ukraine, Russia, Belarus |
| Number of Pages : | 2 |
| Published : | 11/01/2007 |
